分类: 核科学技术 >> 粒子加速器 提交时间: 2023-06-18 合作期刊: 《Nuclear Science and Techniques》
摘要: Microstructure and oxidation behavior of modified Ni-16Mo-7Cr-4Fe alloys by yttrium microalloying were investigated by scanning electron microscopy, transmission electron microscopy, grazing incident X-ray diffraction and synchrotron radiation X-ray fluorescence. M6C and Ni17Y2 phases were observed and the amount of Ni17Y2 increased with yttrium concentration. When the yttrium concentration increased to 0.43wt.%, some Ni17Y2 chains and multi phase regions containing Ni17Y2, M6C and phase appeared, which is harmful for the oxidation resistance. The alloy containing 0.05wt.% yttrium showed the best oxidation resistance, which derives its oxidation resistance from the adequate concentration of yttrium in the solid-solution ( phase), the formation of the protective layer of YCrO3 and chromia oxide and the strengthening effect of yttrium on oxide boundaries.
分类: 核科学技术 >> 粒子加速器 提交时间: 2023-06-18 合作期刊: 《Nuclear Science and Techniques》
摘要: The X-ray diffraction beamline developed at Shanghai Synchrotron Radiation Facility (SSRF)is located at the BL14B1 bending magnet port of the 3.5 GeV storage ring. The beamline optics is based on a collimating mirror, a sagittally focused double crystal monochromator and a focusing mirror. Photon flux of 4.43�1011 phs/s at 10 keV is obtained. The primary instrument equipped in the experimental end-station is a Huber 5021 six-cycle diffractometer. BL14B1 is a general purpose X-ray diffraction beamline and focused on material science, condensed matter physics and other relevant fields looking for structural information.